Taiwan, surrounded by the oceans, is warm and humid. If the indoor temperature is not controlled appropriately, it will give rise to problems. According to related studies, it is indicated that residents are likely to get sick if the indoor relative humidity is over 70 percent. However, if it is lower than 40 percent, it also boosts chances of the survival rate for air-borne viruses and germs. As for indoor molds, they mainly result from air conditioners and indoor materials, especially surfaces of materials. Hence, there is a need to control the humidity, to keep the room clean and dry, to suppress indoor molds and spores, and to find out the moisture distribution of indoor materials and sources of leakage. In so doing, quality of life can be improved. The paper offers an opportunity to conduct an experiment on the moisture distribution of three moisture buffering materials and the humidity of buildings. Measuring instrument for temperature and humidity of Building Materials Surface uses TRAMEX Survey Encounter to measure the moisture content of walls, and the result is put in A Powerful Contouring,Gridding,and Surface Mapping Package for Scientists and Engineers to model the moisture distribution of wall surface materials. i-log is used to test the temperature and humidity. Environmental Chamber allows researchers to test the function of humidity control and to conductexperiments on it. The experiment in the paper indicates that the three construction materials, A-CO, B-SI and C-ES, bring different statistics. However, they are in a standardized test: per square meter, per hour and with one kilogram of each of them. A-CO absorbs moisture 70g/m2and releases moisture 82.3g/m2. B-SI absorbs moisture 61.3g/m2 and releases moisture 51.75g/m2. C-ES absorbs moisture 100g/m2 and releases moisture 91.8g/m2.Therefore, it is clear that the result of moisture absorption goes C-ES>A-CO> B-SI, and that the moisture releasability goes C-ES> A-CO> B-SI. The result and the calibration curve help researchers calculate the formula of the three materials. Hence, the paper is able to provide its readers with the moisture distribution of the above materials and in walls.