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篇名
High-performance liquid chromatographic method for the determination of cloxacillin in commercial preparations and for stability studies
作者 YANN-JEN FANN (YANN-JEN FANN)MEI-CHAI CHENG (MEI-CHAI CHENG)
英文摘要
A reversed-phase column liquid chromatographic method was developed for the assay of cloxacillin and its preparations. The linear calibration range was 0.2-3.0 mg/ml (r=0.9998) and recoveries were generally greater than 99%. The relative standard deviation was 0.13% (n= 10). The high-performance liquid chromatographic assay results were compared with those obtained from a microbiological assay for bulk drug substance, capsule, injection and syrup formulations containing cloxacillin and degraded cloxacillin. At the 99% confidence level, no significant inter-method differences were noted for the paired results. Commercial formulations were also analysed and the results obtained by the proposed method closely agreed with those found by the microbiological method. The results indicated that the proposed method is a suitable substitute for the microbiological method for assays and stability studies of cloxacillin preparations.
起訖頁 140-145
刊名 藥物食品檢驗局調查研究年報  
期數 1992 (10期)
出版單位 衛生福利部食品藥物管理署
該期刊-上一篇 本省東部特產(鴨賞及膽肝)與香腸中防腐劑及保色劑使用現況調查
該期刊-下一篇 Determination of Dicloxacillin Preparations by Liquid Chromatography
 

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